Vinyl Acetate → HCID 86755500, compound

Participants

Reaction Conditions

Reaction Steps

A 19:6:75 mole ratio poly(vinyl acetate/acrylic acid/methyl acrylate) was synthesized in the following manner. In a liter polymerization flask fitted with baffles, 295.0 g of deionized water, 10.34 of nonylphenol ethoxylate sulfate ammonium salt (58% solution), available from Rhone-Poulenc of Cranbury, N.J., 9.02 g of sodium dodecyl benzene sulfonate (23% solution) available from Rhone-Poulenc of Cranbury, N.J., 2.0 of EO-PO block copolymer available from BASF, Mt. Olive, N.J. were taken and a solution was effected by mixing. To the resultant clear solution, 0.19 g of SAG 2001, an antifoam available from Witco of Greenwich, Conn. and vinyl acetate (99%) 40.8 g was added, nitrogen was sparged through the solution for 15 minutes and the solution was cooled down to 10° C.

Provenance & Evidence