HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86755502, compound → HCID 86755505, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86755502 | HCID 86755502 | — |
| Reactant | HCID 86755506 | HCID 86755506 | — |
| Product | HCID 86755505 | HCID 86755505 | 35% |
Reaction Steps
Operating as in Example 2, but employing 6-methyl-8β-[5-(5-bromo-pyridin-3-yl)-1,3,4-thiadiazol-5-yl]-10α-methoxy-ergoline instead 6-methyl-8β-methy-[5-(5-bromo-pyridin-3-yl)-1,2,4-oxadiazol-3-yl]-10α-methoxy-ergoline, the title compound was obtained in 35% yield, m.p.131-137° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06087371 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-491b87772deb4438a29454ac40acc07f |
| Source note | uspto-grants-2000_07 |