HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 56626166, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 56614900 | HCID 56614900 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 56626166 | HCID 56626166 | 77.3% |
Reaction Steps
90 mg of compound (5) was dissolved in 2.2 ml of methanol and stirred together with 121 μl of 1N NaOH for 2 hours under cooling with ice. After addition of water, the reaction solution was extracted with ethyl acetate, and the ethyl acetate extract was dried over anhydrous sodium sulfate and concentrated in vacuo to dryness to give 66 mg of compound (6) as a colorless powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06087390 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-e699c0d5e99b4c869577f79df9de681c |
| Source note | uspto-grants-2000_07 |