HCID 56609779, compound → HCID 18703971, compound

Participants

Reaction Steps

21.2 mg of compound (28) was dissolved in 6 ml of ethyl acetate and stirred together with a catalytic amount of 10% palladium-carbon under a hydrogen atmosphere at room temperature for 50 minutes. The reaction solution was filtered, and the filtrate was concentrated in vacuo. The reaction product was dissolved in 4 ml of methanol and washed with 4 ml of n-hexane twice. The methanol layer was concentrated in vacuo to give 10.0 mg of compound (29) as a colorless oily substance.

Provenance & Evidence