HCID 56618635, compound → HCID 18703956, compound

Participants

Reaction Steps

13.0 mg of compound (58) was dissolved in 2 ml of ethyl acetate and stirred together with a catalytic amount of 10% palladium-carbon under a hydrogen atmosphere at room temperature. After 30 minutes, the reaction solution was filtered and concentrated in vacuo. The reaction product was dissolved in 2 ml of methanol and washed with 2 ml of n-hexane twice, and the lower layer was concentrated in vacuo to give 6.6 mg of compound (59) as a colorless solid.

Provenance & Evidence