HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 18412514, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ammonium Carbonate | HCID 517111 | — |
| Reactant | HCID 18412367 | HCID 18412367 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18412514 | HCID 18412514 | 73% |
Reaction Steps
Prepared analogously to Example 25d from 1-methyl-2-[2-(4-cyanophenyl)ethyl]-benzimidazol-5-yl-carboxylic acid-N-phenyl-N-(ethoxycarbonylmethyl)-amide and ethanolic hydrochloric acid, ethanol and ammonium carbonate. Yield: 73% of theory, Rf value: 0.15 (silica gel; dichloromethane/ethanol=4:1) C28H29N5O3 (483.6) ##EQU19##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06087380 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-4cd364a39ef7420aa9dc0a771e23d75c |
| Source note | uspto-grants-2000_07 |