HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbonochloridic acid, cyclohexyl ester → HCID 140443500, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbonochloridic acid, cyclohexyl ester | HCID 83262 | — |
| Reactant | HCID 18412394 | HCID 18412394 | — |
| Solvent | Dichloromethane ethanol | HCID 21584144 | — |
| Product | HCID 140443500 | HCID 140443500 | 40% |
Reaction Steps
Prepared analogously to Example 90 from 1-methyl-2-[N-(4-amidinophenyl)-aminomethyl]-benzimidazol-5-yl-carboxylic acid-N-(2-pyridyl)-N-methoxycarbonylmethyl-amide-hydrochloride and cyclohexyl chloroformate. Yield: 40% of theory, C32H35N7O5 (597.7) Rf value: 0.26 (silica gel; dichloromethane/ethanol=19:1) ##EQU85##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06087380 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-67de48978b7c49c1b1915cb4cb58fe58 |
| Source note | uspto-grants-2000_07 |