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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2288460Generated: October 31, 2026

Methyl chloroformate → HCID 140409612, compound

https://huagongshe.com/reaction/2288460

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl chloroformateHCID 6586—
Reactant1-methyl-2-[N-(4-amidinophenyl)aminomethyl]benzimidazol-5-yl-carboxylic acid-N-(2-pyridyl)-N-ethoxycarbonylmethylamide hydrochlorideHCID 18412300—
SolventDichloromethane ethanolHCID 21584144—
ProductHCID 140409612HCID 14040961262%

Reaction Steps

Prepared analogously to Example 90 from 1-methyl-2-[N-(4-amidinophenyl)-aminomethyl]-benzimidazol-5-yl-carboxylic acid-N-(2-pyridyl)-N-ethoxycarbonylmethyl-amide-hydrochloride and methyl chloroformate. Yield: 62% of theory, C28H29N7O5 (543.6) Rf value: 0.19 (silica gel; dichloromethane/ethanol=19:1) ##EQU86##

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06087380
Source datasetuspto-grants-2000_07
ORD IDord-ed8b18e03942487facd229bd698f6c6d
Source noteuspto-grants-2000_07