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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2288532Generated: November 1, 2026

Benzyl chloroformate → HCID 140409598, compound

https://huagongshe.com/reaction/2288532

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzyl chloroformateHCID 10387—
ReactantEthyl 3-(2-(((4-carbamimidoylphenyl)amino)methyl)-1-methyl-N-(pyridin-2-yl)-1H-benzo(d)imidazole-5-carboxamido)propanoate hydrochlorideHCID 18412337—
SolventDichloromethane methanolHCID 21226129—
ProductHCID 140409598HCID 14040959864%

Reaction Steps

Prepared analogously to Example 90 from 1-methyl-2-[N-(4-amidinophenyl)-aminomethyl]-benzimidazol-5-yl-carboxylic acid-N-(2-pyridyl)-N-(2-ethoxycarbonylethyl)-amide-hydrochloride and benzyl chloroformate. Yield: 64% of theory, C35H35N7O5 (633.6) Rf value: 0.60 (silica gel; dichloromethane/methanol=9:1) ##EQU131##

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06087380
Source datasetuspto-grants-2000_07
ORD IDord-5ad1b2af07264ede82b0268e7cd3bb29
Source noteuspto-grants-2000_07