HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexyl chloroformate → HCID 140409624, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexyl chloroformate | HCID 22466 | — |
| Reactant | HCID 18412432 | HCID 18412432 | — |
| Solvent | Dichloromethane ethanol | HCID 21584144 | — |
| Product | HCID 140409624 | HCID 140409624 | 73% |
Reaction Steps
Prepared analogously to Example 90 from 1-methyl-2-[N-(4-amidinophenyl)-aminomethyl]-benzimidazol-5-yl-carboxylic acid-N-phenyl-N-(3-benzyloxy-n-propyl)-amide-hydrochloride and n-hexyl chloroformate. Yield: 73% of theory, C40H46N6O4 (674.9) Rf value: 0.46 (silica gel; dichloromethane/ethanol=9:1) ##EQU135##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06087380 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-505b14ff295049baaeeecf939938bc91 |
| Source note | uspto-grants-2000_07 |