HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanethiol → HCID 21702001, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanethiol | HCID 6343 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | HCID 21702003 | HCID 21702003 | — |
| Product | HCID 21702001 | HCID 21702001 | 29% |
Reaction Steps
[6-Methoxy-2-(4-methoxyphenyl)benzo[b]thiophen-3-yl][4-(Acetoxymethoxy)phenyl]methanone (1.7 g, 2.5 mmol) was converted to the title compound by the procedure of Example 3 using 500 mg (7.5 mmol) of ethanethiol and 1.0 g (7.5 mmol) of aluminum chloride except that the total reaction time was 4 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06090843 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-26d91f0731ed4ad8a1b9a176d85165d3 |
| Source note | uspto-grants-2000_07 |