HuagongsheHuagongshe Chemistry Print Report · For research reference only
N5-(iminomethoxymethyl)-L-ornithine dihydrochloride → HCID 178475098, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N5-(iminomethoxymethyl)-L-ornithine dihydrochloride | HCID 86583873 | — |
| Reactant | HCID 178475097 | HCID 178475097 | — |
| Product | HCID 178475098 | HCID 178475098 | 94% |
Reaction Steps
By the method described above for the preparation of N5 -(iminomethoxymethyl)-L-ornithine dihydrochloride, 0.78 g (1.97 mmol) N2 -(tert-butoxycarbonyl)-N5 -(ethoxyiminomethyl)-L-ornithine tert-butyl ester hydrochloride was deprotected to yield 0.51 g (94%) N5 -(ethoxyiminomethyl)-L-ornithine dihydrochloride monohydrate. TLC (silica gel, ammonium hydroxide:methanol/1:25) Rf=0.24. Mass spectrum (CI) 204 (MH+, 74%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06090846 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-bce4a124f2594d5d987e0661bbe41549 |
| Source note | uspto-grants-2000_07 |