HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69967351, compound → HCID 136333675, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69967351 | HCID 69967351 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 136333675 | HCID 136333675 | — |
Reaction Steps
A solution of 3-methoxy-6-benzyloxy-7-propylbenz-(4,5)-isoxazole (Step E; 181 mg) in ethyl acetate (4 mL) was treated with 10% palladium on carbon catalyst (25 mg). The mixture was shaken under a hydrogen atmosphere (40 psi) for 3 hours. The mixture was filtered through Celite and concentrated to a solid. The title compound was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06090836 |
| Source dataset | uspto-grants-2000_07 |
| ORD ID | ord-fa808d11775b45f48ebf3dd91f1f4a3b |
| Source note | uspto-grants-2000_07 |