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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2289089Generated: October 30, 2026

HCID 69967351, compound → HCID 136333675, compound

https://huagongshe.com/reaction/2289089

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 69967351HCID 69967351—
CatalystPalladiumHCID 23938—
SolventEthyl AcetateHCID 8857—
ProductHCID 136333675HCID 136333675—

Reaction Steps

A solution of 3-methoxy-6-benzyloxy-7-propylbenz-(4,5)-isoxazole (Step E; 181 mg) in ethyl acetate (4 mL) was treated with 10% palladium on carbon catalyst (25 mg). The mixture was shaken under a hydrogen atmosphere (40 psi) for 3 hours. The mixture was filtered through Celite and concentrated to a solid. The title compound was used without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06090836
Source datasetuspto-grants-2000_07
ORD IDord-fa808d11775b45f48ebf3dd91f1f4a3b
Source noteuspto-grants-2000_07