Sulfuric Acid → HCID 2724782, compound

Participants

Reaction Conditions

Reaction Steps

DCG was prepared according to the procedure described in J. Am. Chem. Soc., 1949, 71, 3072. A mixture of 90 g of α-D-glucose, 200 mL of cyclohexanone and 13 mL of sulfuric acid was allowed to stir at 20° C. for 12 h to afford 43.9 g (29%) of the above-titled compound, after two crystallizations: mp.=130.5-131.5° C. (lit. 131.1-132.4° C.).

Provenance & Evidence