Pyridine → HCID 69317115, compound

HRID 2289175Notes

Reaction equation

[OH:1][CH2:2][CH:3]1[CH2:8][CH2:7][CH:6]([OH:9])[CH2:5][CH2:4]1.[C:10](OC(=O)C)(=[O:12])[CH3:11].N1C=CC=CC=1>>[C:10]([O:1][CH2:2][CH:3]1[CH2:8][CH2:7][CH:6]([OH:9])[CH2:5][CH2:4]1)(=[O:12])[CH3:11]

Participants

Reactant 3

HCID 1049Pyridine

HCID 7918Acetic Anhydride

HCID 12892866Rac-(1s,4s)-4-(hydroxymethyl)cyclohexanol

Product 1

HCID 69317115HCID 69317115, compound

Procedure

The 4-(hydroxymethyl)cylohexan-1-ol obtained above is treated with 1 eq. of acetic anhydride and 2 eq. of pyridine to provide 4-acetoxymethylcylohexan-1-ol.

Sources & evidence

ORD record: ord-bebb1664c01b43068610b7bb8b41c299
Source dataset: uspto-grants-2000_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06090950

Reaction notes

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