Pyridine → HCID 178510973, compound

Participants

Reaction Steps

To a suspension of the title compound of Example 89 (0.11 g) in 25 mL EtOAc is added triethylamine (0.08 mL) and pyridine (5 mL) to aid dissolution. After 10% Pd/C (50 mg) is added, the reaction is placed under a hydrogen balloon. After 2 hours, the reaction is complete and subsequently filtered over Celite. The filter cake is washed with ethyl acetate. The filtrate is concentrated to give a tan solid which is further dried on the vacuum pump to afford the desired product (0.088 g).

Provenance & Evidence