HCID 178454811, compound → HCID 178522911, compound

Participants

Reaction Steps

A solution of 95 mg of compound of Example 267 (F-2 wherein X=CH2 and Y=F) in 1 mL of 1:1 TFA-dichloromethane is stirred for 30 min, then added dropwise to 50 mL of rapidly stirred 2:1 ether-hexane. The solid is filtered off, washed with hexane, and dried under vacuum to provide 65 mg of the title compound as a white solid.

Provenance & Evidence