HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 13520695, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | 3,4-Dimethoxy-1,2-benzenediacetonitrile | HCID 10036245 | — |
| Product | HCID 13520695 | HCID 13520695 | — |
Reaction Steps
An amount of 3.7 gm (0.017 mol) of 3,4-dimethoxy-o-phenylenediacetonitrile is suspended in 10 ml of glacial acetic acid and then combined at 20° C. with 12 ml of 30% hydrobromic acid in glacial acetic acid. The mixture is stirred for a further three hours at ambient temperature, and the precipitate is subjected to suction filtration, washed with glacial acetic acid and then with acetone/ether, and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04616011 |
| Source dataset | uspto-grants-1986_10 |
| ORD ID | ord-5ffb6f2149a944f3a2e2b3cfcd21e62e |
| Source note | uspto-grants-1986_10 |