Thiazolidinedione → HCID 13731109, compound
Reaction equation
Cl[CH:2]([C:7]1[CH:12]=[C:11]([Cl:13])[CH:10]=[C:9]([CH3:14])[C:8]=1[O:15][CH3:16])[C:3]([O:5]C)=[O:4].S1CC(=[O:22])NC1=O>>[OH:22][CH:2]([C:7]1[CH:12]=[C:11]([Cl:13])[CH:10]=[C:9]([CH3:14])[C:8]=1[O:15][CH3:16])[C:3]([OH:5])=[O:4]Participants
3
Procedure
It was converted to methyl alpha-chloro-alpha-(5-chloro-2-methoxy-3-methylphenyl)acetate by the chlorination/esterification procedure of Preparation A. The product was used directly to prepare the thiazolidine-2,4-dione of Example 4.
Sources & evidence
- ORD record
- ord-3ba5be34f28c40a49d1b8473841a7a8b
- Source dataset
- uspto-grants-1986_10
- Patent number
- US04617312
Reaction notes
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