HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → 3-Methoxy-4-(2-thienyl)benzenamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Thiophene, 2-(2-methoxy-4-nitrophenyl)- | HCID 13768627 | — |
| Catalyst | Iron | HCID 23925 | — |
| Solvent | Water | HCID 962 | — |
| Product | 3-Methoxy-4-(2-thienyl)benzenamine | HCID 13768628 | 86.1% |
Reaction Steps
In a manner similar to Example 1, Step B, the reaction of 6.6 g (0.03 mole) of 2-(2-methoxy-4-nitrophenyl)thiophene, 13.65 g (0.24 mole) of iron powder and 25.2 g (0.42 mole) of glacial acetic acid in 36 ml of water produced 5.3 g of 3-methoxy-4-(thien-2-yl)aniline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04617316 |
| Source dataset | uspto-grants-1986_10 |
| ORD ID | ord-2ab402ca6e6d4fbda7b7cad66a1e7502 |
| Source note | uspto-grants-1986_10 |