Dichloromethane ethyl acetate methanol → HCID 57049758, compound

HRID 2290580Notes

Reaction equation

HRID 2290580 reaction equation
[O:1]=[C:2]([N:17]1[CH2:22][CH:21]=[C:20]([C:23]2[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=2)[CH2:19][CH2:18]1)[CH2:3][S:4][CH2:5][C:6]1[C:14]2[C:9](=[CH:10][CH:11]=[C:12](OC)[CH:13]=2)[NH:8][CH:7]=1.[CH2:29](Cl)Cl.CO.C(OCC)(=O)C>>[O:1]=[C:2]([N:17]1[CH2:22][CH:21]=[C:20]([C:23]2[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=2)[CH2:19][CH2:18]1)[CH2:3][S:4][CH2:5][C:6]1[C:14]2[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=2)[NH:8][C:7]=1[CH3:29]

Participants

3

Reactant 2

HCID 21901258Dichloromethane ethyl acetate methanolHCID 57279427HCID 57279427, compound

Product 1

HCID 57049758HCID 57049758, compound

Procedure

3-[4-oxo-4-(4-phenyl-1,2,3,6-tetrahydropyridyl)-2-thiabutyl]-5-methoxyindole, Rf 0.78 (CH2Cl2 /methanol/ethyl acetate 7:2:1)

Sources & evidence

ORD record
ord-53a1b5ed49a541be97560caa43c71bfc
Source dataset
uspto-grants-1986_10
Patent number
US04617309

Reaction notes

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