HCID 23078577, compound → HCID 23078281, compound

Participants

Reaction Steps

(4,5-Dimethylfuran-2-yl)-(4-methylpyridin-3-yl)-methanol (174 mg) was dissolved in chloroform (5 ml) to prepare a solution. Manganese dioxide (1.05 g) was added to the solution, and the mixture was stirred at room temperature overnight. The reaction solution was then filtered through Celite. The solvent was removed from the filtrate by distillation under the reduced pressure. The residue was purified by column chromatography using hexane-ethyl acetate to give (4,5-dimethylfuran-2-yl)-(4-methylpyridin-3-yl)-methanone (151 mg, yield 88%).

Provenance & Evidence