Hydrochloric Acid → HCID 13745944, compound

Participants

Reaction Steps

The compound of Example 10 (25 mg) was dissolved in 1N NaOH (0.2 ml) and THF (1 ml). The reaction mixture was stirred at room temperature for 1.5 hours. The reaction was poured into a mixture of ice and dilute HCl and extracted with ethyl acetate. The combined organic extracts were dried and evaporated to yield the title compound which was recrystallized from ether-hexane, m.p. 129°-129.5°.

Provenance & Evidence