1,3-Propanediamine → HCID 20229969, compound

HRID 2290698Notes

Reaction equation

HRID 2290698 reaction equation
C(S[C:4](=[S:16])[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15])C.[NH2:17][CH2:18][CH2:19][CH2:20][NH2:21]>C1(C)C=CC=CC=1>[NH2:17][CH2:18][CH2:19][CH2:20][NH:21][C:4](=[S:16])[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15]

Participants

4

Reactant 2

HCID 4281,3-PropanediamineHCID 12863223HCID 12863223, compound

Product 1

HCID 20229969HCID 20229969, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent2×

Conditions

Temperature
10 °C

Procedure

10.4 g of ethyl-dodecanedithioate is dissolved in 100 ml of toluene and the solution obtained is mixed with a solution of 30 g of 1,3-diaminopropane in 200 ml of toluene. The mixture is maintained at about 10° C. for 1 hour, with stirring.

Workup

  1. customthe solution obtained

Sources & evidence

ORD record
ord-0f4083ef5c1345e6b88c347dda4b86fa
Source dataset
uspto-grants-1986_10
Patent number
US04618416

Reaction notes

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