HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 3695481, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | HCID 3631643 | HCID 3631643 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 3695481 | HCID 3695481 | — |
Reaction Steps
5.0 g (0.03 mol) of 1-hydroxymethyl-5-methylbenzotriazole and 2.9 g (0.03 mol) of aniline were suspended in ethanol and refluxed for 1 hour. The insoluble substance was removed by filtration while it was still hot and the filtrate was cooled to obtain crude crystals. By recrystallization of the crude crystals from ethanol 4.2 g of the desired compound having a melting point of 149° to 152° C. was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04618563 |
| Source dataset | uspto-grants-1986_10 |
| ORD ID | ord-9f7eaee3063c4c6d95a25822e5a8c5b6 |
| Source note | uspto-grants-1986_10 |