Thiosemicarbazide → HCID 136332168, compound

HRID 2290730Notes

Reaction equation

HRID 2290730 reaction equation
[C:1]([NH:4][C:5]1[CH:6]=[C:7]([C:12](=O)[C:13](=[N:15][OH:16])[CH3:14])[CH:8]=[CH:9][C:10]=1[Cl:11])(=[O:3])[CH3:2].[NH2:18][NH:19][C:20]([NH2:22])=[S:21]>>[C:1]([NH:4][C:5]1[CH:6]=[C:7]([C:12](=[N:18][NH:19][C:20]([NH2:22])=[S:21])[C:13](=[N:15][OH:16])[CH3:14])[CH:8]=[CH:9][C:10]=1[Cl:11])(=[O:3])[CH3:2]

Participants

3

Reactant 2

HCID 2723789ThiosemicarbazideHCID 73666223HCID 73666223, compound

Product 1

HCID 136332168HCID 136332168, compoundYield 92.6%

Procedure

3'-Acetamido-4'-chloro-2-hydroxyiminopropiophenone (70.75 g) was reacted with thiosemicarbazide (28.4 g) in the same manner as Example 1-(1) to give 3'-acetamido-4'-chloro-2-hydroxyiminopropiophenone thiosemicarbazone (84.36 g).

Sources & evidence

ORD record
ord-252b6a84e0c64edf8ac8a8898c81fb68
Source dataset
uspto-grants-1986_10
Patent number
US04618610

Reaction notes

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