Phenyl isocyanate → HCID 13386050, compound

HRID 2290734Notes

Reaction equation

HRID 2290734 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[CH:9]([CH3:15])[NH:10][C:11](=[O:14])[NH:12][N:13]=2)=[CH:4][CH:3]=1.[C:16]1([N:22]=[C:23]=[O:24])[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1>>[C:16]1([NH:22][C:23](=[O:24])[NH:1][C:2]2[CH:3]=[CH:4][C:5]([C:8]3[CH:9]([CH3:15])[NH:10][C:11](=[O:14])[NH:12][N:13]=3)=[CH:6][CH:7]=2)[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1

Participants

3

Reactant 2

HCID 7672Phenyl isocyanateHCID 133860336-(4-aminophenyl)-5-methyl-4,5-dihydro-1,2,4-triazin-3(2H)-one

Product 1

HCID 13386050HCID 13386050, compound

Procedure

6-(4-Aminophenyl)-5-methyl-4,5-dihydro-1,2,4-triazin-3(2H)-one (1.5 g) was reacted with phenyl isocyanate (0.88 ml) in the same manner as Example 6 to give 6-[4-(3-phenylureido)phenyl]-5-methyl-4,5-dihydro-1,2,4-triazin-3(2H)-one (1.26 g).

Sources & evidence

ORD record
ord-ceaf2a0d50ae48e3a4f016cc045bb877
Source dataset
uspto-grants-1986_10
Patent number
US04618610

Reaction notes

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