p-Toluenesulfonic acid → HCID 54413729, compound

Participants

Reaction Steps

A mixture of 1.4 g of 1-(3,4-dibenzyloxyphenyl)-9-ethylenedioxy-1-decene, 50 ml of acetone, and 50 mg of p-toluenesulfonic acid was stirred overnight at room temperature. After adding thereto 50 mg of sodium carbonate, the reaction mixture was concentrated under reduced pressure, and after adding thereto 50 ml of water, the product was extracted with toluene. The extract was washed with water, dried over anhydrous magnesium sulfate, and concentrated under reduced pressure to provide 1.1 g of 1-(3,4-dibenzyloxyphenyl)-1-decen-9-one as an oil.

Provenance & Evidence