HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13519329, compound → HCID 20230500, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13519329 | HCID 13519329 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20230500 | HCID 20230500 | 93.9% |
Reaction Steps
In 10 ml of ethanol was dissolved 0.5 g of 1-(3,4-dibenzyloxyphenyl)-2-decanol and the compound was catalytically reduced using 0.2 g of 10% palladium-carbon at room temperature and under atomospheric until the absorption of hydrogen stopped. After the reaction was over, the catalyst was filtered off and the filtrate was concentrated under reduced pressure to provide 0.28 g of 1-(3,4-dihydroxyphenyl)-2-decanol. Oily product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04618627 |
| Source dataset | uspto-grants-1986_10 |
| ORD ID | ord-899d31f0088e460dbbee34a9c0dc35e7 |
| Source note | uspto-grants-1986_10 |