HCID 54182095, compound → HCID 20230517, compound

Participants

Reaction Steps

Using 0.1 g of 10% palladium-carbon as catalyst, 560 mg of 1-(3,4-dibenzyloxyphenyl)-3-methoxy-4-methyl-1-octene was catalytically reduced in a mixture of 5 ml of methanol and 5 ml of ethyl acetate until the absorption of hydrogen stopped. Thereafter, the catalyst was filtered off and the filtrate was concentrated under reduced perssure to provide 330 mg of oily 1-(3,4-dihydroxyphenyl)-3-methoxy-4-methyl-octane.

Provenance & Evidence