HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 178418555, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Butylphenyl isocyanate | HCID 2796313 | — |
| Reactant | 3-[4-(4-Chlorophenethyl)piperazin-1-yl]propanethiol dihydrochloride | HCID 13731126 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178418555 | HCID 178418555 | 49.7% |
Reaction Steps
The procedure described in Example 2 was followed, using 1.4 g of 4-n-butylphenyl isocyanate, 3.0 g of 3-[4-(4-chlorophenethyl)piperazin-1-yl]propanethiol dihydrochloride, 0.8 g of triethylamine and 50 ml of methylene chloride, to give 1.1 g (25% of theory) of N-(4-n-butylphenyl)-S-{3-[4-(4-chlorophenethyl)piperazin-yl]propyl}thiocarbamate dihydrochloride as a white crystalline solid, M.p. 252°-254° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04618677 |
| Source dataset | uspto-grants-1986_10 |
| ORD ID | ord-07b65006de644e9e9ded06908a6d010c |
| Source note | uspto-grants-1986_10 |