HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 178418514, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Butylphenyl isocyanate | HCID 2796313 | — |
| Reactant | 3-{4-[3-(4-Chlorophenyl)propyl]piperazin-1-yl}propanethiol dihydrochloride | HCID 13731130 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178418514 | HCID 178418514 | — |
Reaction Steps
The procedure described in Example 2 was followed, using 2.5 g of 4-n-butylphenyl isocyanate, 5.0 g of 3-{4-[3-(4-chlorophenyl)propyl]piperazin-1-yl}propanethiol dihydrochloride, 1.4 g of triethylamine and 50 ml of methylene chloride, to give 2.7 g (34% of theory) of N-(4-n-butylphenyl-S-{3-[4-[3-(4-chlorophenyl)propyl]piperazin-1-yl]propyl}thiocarbamate dihydrochloride as a white crystalline solid, m.p. 270°-272° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04618677 |
| Source dataset | uspto-grants-1986_10 |
| ORD ID | ord-a7d538926ab34bd69059f7b135992603 |
| Source note | uspto-grants-1986_10 |