HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexyl isocyanate → HCID 178418556, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexyl isocyanate | HCID 75659 | — |
| Reactant | 3-{4-[4-(4-Chlorophenyl)butyl]piperazin-1-yl}propanethiol | HCID 13731133 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178418556 | HCID 178418556 | 99.8% |
Reaction Steps
The procedure described in Example 2 was followed, using 1.0 g of n-hexyl isocyanate, 2.6 g of 3-{4-[4-(4-chlorophenyl)butyl]piperazin-1-yl}propanethiol and 25 ml of methylene chloride, to give 1.4 g (32% of theory) of N-(n-hexyl)-S-{3-[4-[4-(4-chlorophenyl)butyl]piperazin-1-yl]propyl}thiocarbamate dihydrochloride as a white crystalline solid, M.p. 235°-245° C. (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04618677 |
| Source dataset | uspto-grants-1986_10 |
| ORD ID | ord-27a2a2bcae87453cb7afe6a4bf1764fe |
| Source note | uspto-grants-1986_10 |