HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl iodide → HCID 86234905, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl iodide | HCID 10962 | — |
| Reactant | Disodium | HCID 141233 | — |
| Reactant | N,N'-Dicyanoadipamide | HCID 3015775 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | HCID 86234905 | HCID 86234905 | — |
Reaction Steps
Analogously to Example 3, 23.8 g (0.1 mol) of the disodium salt of adipic acid bis-(N-cyanamide) and 55.2 g (0.2 mol+50% excess) of n-butyl iodide are reacted in 50 ml of N-methylpyrrolidone at 92°-100° C. for 5 hours and 15 minutes and the mixture is worked up.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04618712 |
| Source dataset | uspto-grants-1986_10 |
| ORD ID | ord-4de6d2b01a884c658e2b37053d8d54d5 |
| Source note | uspto-grants-1986_10 |