HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diphenylphosphine → Docosyl(diphenyl)phosphane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diphenylphosphine | HCID 70017 | — |
| Reactant | 1-Docosene | HCID 74138 | — |
| Product | Docosyl(diphenyl)phosphane | HCID 13750329 | 96% |
Reaction Steps
In a manner similar to Example 1, docosene (obtained from Aldrich) and diphenylphosphine were reacted under nitrogen at 250° C. for 27 hours. Removal of unreacted olefin and diphenylphosphine by vacuum distillation gave docosyldiphenylphosphine. The yield was 96% based on recovered olefin. The conversion was 57% based on recovered olefin.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04618719 |
| Source dataset | uspto-grants-1986_10 |
| ORD ID | ord-22e3d7ed4f8945b8a226be3114097bd2 |
| Source note | uspto-grants-1986_10 |