HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2290985Generated: October 31, 2026
Azobisisobutyronitrile → Methyl Methacrylate
https://huagongshe.com/reaction/2290985
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | Methyl Methacrylate | HCID 6658 | — |
| Reactant | Glycol monoethyl ether | HCID 8076 | — |
| Reactant | 2-Hydroxyethyl Methacrylate | HCID 13360 | — |
| Product | Methyl Methacrylate | HCID 6658 | — |
| Product | 2-Hydroxyethyl Methacrylate | HCID 13360 | — |
| Product | 2-(Oxiran-2-yl)ethyl 2-methylprop-2-enoate | HCID 21727127 | — |
Reaction Steps
To 140 g of ethyl cellosolve were added 42 g of 3,4-epoxybutyl methacrylate⟦,9⟧, 9 g of methyl methacrylate, 9 g of hydroxyethyl methacrylate and 0.3 g of AIBN. The mixture was gently stirred and heated up to 90° C. During this treatment, nitrogen was continuously blown into the reaction system for more than about four hours. Consequently obtained was a light yellow solution measuring approximately 80 CPS in viscosity (molecular weight about 18,000). Thus a copolymer of 3,4-epoxybutyl methacrylate, methyl methacrylate and hydroxyethyl methacrylate was formed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | USRE032272 |
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| Source dataset | uspto-grants-1986_10 |
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| ORD ID | ord-ff4db803c49f43399aed17529bcf0ea0 |
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| Source note | uspto-grants-1986_10 |
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