HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12803422, compound → 1-(2-Methoxyethyl)-4-phenylimidazolidin-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12803422 | HCID 12803422 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-(2-Methoxyethyl)-4-phenylimidazolidin-2-one | HCID 12803423 | — |
Reaction Steps
Approximately 10.9 g. of 1-(2-methoxyethyl)-4-phenyl-4-imidazolin-2-one and 1 g. of 10% palladium on carbon in 100 ml. of ethanol is hydrogenated in a Parr Shaker apparatus at 30 psig of hydrogen for 45 minutes. The catalyst is filtered, washed with ethanol, and the filtrate is concentrated to give the title compound as a waxy white solid; m.p. 82°-83° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04620009 |
| Source dataset | uspto-grants-1986_10 |
| ORD ID | ord-99ae5f79d65746aab7f858f6a2696ef2 |
| Source note | uspto-grants-1986_10 |