HCID 20229663, compound → HCID 20229653, compound

HRID 2291137Notes

Reaction equation

HRID 2291137 reaction equation
[CH2:1]([O:5][CH2:6][CH2:7][N:8]1[CH:12]=[C:11]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[NH:10][C:9]1=[O:19])[CH2:2][CH2:3][CH3:4].[H][H]>C(O)C.[Pd]>[CH2:1]([O:5][CH2:6][CH2:7][N:8]1[CH2:12][CH:11]([C:13]2[CH:14]=[CH:15][CH:16]=[CH:17][CH:18]=2)[NH:10][C:9]1=[O:19])[CH2:2][CH2:3][CH3:4]

Participants

5

Reactant 2

HCID 20229663HCID 20229663, compoundHCID 178418361HCID 178418361, compound

Product 1

HCID 20229653HCID 20229653, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent

Procedure

A solution of 1-(2-butoxyethyl)-4-phenyl-4-imidazolin-2-one in ethanol with 10% palladium on carbon catalyst is reduced in an atmosphere of hydrogen. After the theoretical amount of hydrogen is absorbed, the catalyst is filtered and filtrate concentrated to give the title compound.

Workup

  1. customAfter the theoretical amount of hydrogen is absorbed
  2. filtrationthe catalyst is filtered
  3. concentrationfiltrate concentrated

Sources & evidence

ORD record
ord-261c820b65d9407ead44c4da30b2b7d1
Source dataset
uspto-grants-1986_10
Patent number
US04620009

Reaction notes

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