HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methyl-2-butenoic acid → Benzene, ((3-methyl-2-butenyl)oxy)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methyl-2-butenoic acid | HCID 10931 | — |
| Reactant | 3-Methyl-2-buten-1-OL | HCID 11173 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | Phenolate Sodium | HCID 4445035 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | Benzene, ((3-methyl-2-butenyl)oxy)- | HCID 564931 | — |
Reaction Steps
3,3-dimethylallylphenyl ether was prepared from 3,3-dimethylacrylic acid by reduction with sodium dihydro-bis (2-methoxyethoxy) aluminate in benzene, chlorination of the resulting 3,3-dimethylallyl alcohol with thionyl chloride and reaction of the product with sodium phenoxide in the presence of a polar solvent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04795639 |
| Source dataset | uspto-grants-1989_01 |
| ORD ID | ord-35451352efb54ffba49775c255a6329a |
| Source note | uspto-grants-1989_01 |