HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2291426Generated: October 26, 2026
m-Chloroperbenzoic acid → 4-(4,5-Epoxypentoxy)-4'-nitrobiphenyl
https://huagongshe.com/reaction/2291426
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | 4-(4-Pentenoxy)-4'-nitrobiphenyl | HCID 19901284 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 4-(4,5-Epoxypentoxy)-4'-nitrobiphenyl | HCID 22163019 | — |
Reaction Steps
To 250 ml of methylene chloride is added 28.3 g of 4-(4-penteneoxy)-4'-nitrobiphenyl. The solution is cooled to 0° C., and 18 g of meta-chloroperbenzoic acid is added slowly. The mixture is stirred at 0° C. for 24 hours, and allowed to warm to room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04796976 |
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| Source dataset | uspto-grants-1989_01 |
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| ORD ID | ord-babd60ad0e80441ba470f984e20547fc |
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| Source note | uspto-grants-1989_01 |
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