Isopropylamine → HCID 14013800, compound

Participants

Reaction Steps

This compound was prepared as described in Example 37: 7.0 g (0.018 mol) of product of Example 27, 3.2 ml (0.037 mol) of isopropylamine in 30 ml of DMF were reacted at room temperature for 1/2 hour affording a brown oil which was kugelrohr distilled at Pa, pot temperature 95° C., to give 6.07 g (83.8%) of product as a yellow oil, nD25 1.4560.

Provenance & Evidence