HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → HCID 14013802, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | HCID 14013761 | HCID 14013761 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 14013802 | HCID 14013802 | — |
Reaction Steps
This compound was prepared as described in Example 37: 6.0 g (0.016 mol) of product of Example 27, 2.6 ml (0.032 mol) of pyrrolidine in 30 ml of DMF were reacted affording a brown solid which was recrystallized in hot hexane giving 5.18 g (78.1%) of product as a tan solid; mp 68.5°-70° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04797149 |
| Source dataset | uspto-grants-1989_01 |
| ORD ID | ord-46a694ef18964d06a75eb8dbeeb05a7a |
| Source note | uspto-grants-1989_01 |