反应详情

To 5 g of 4,4-dimethyl-cyclohexylcarboxylic acid was added an excess of thionyl chloride, and the mixture was heated with stirring for 3 hours. After the reaction, the remaining thionyl chloride was distilled off in a vacuum, 10 ml of benzene was added to the residue and the mixture was distilled in a vacuum, giving oily 4,4-dimethylcyclohexylcarbonyl chloride.

1. temperaturethe mixture was heated
2. customAfter the reaction
3. distillationthe remaining thionyl chloride was distilled off in a vacuum, 10 ml of benzene
4. additionwas added to the residue
5. distillationthe mixture was distilled in a vacuum