Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethyl Sulfoxide → HCID 14326857, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethyl Sulfoxide | HCID 679 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | Oxalyl chloride | HCID 65578 | — |
| 반응물 | 1-(5-Isoquinolinesulfonyl)-3-hydroxy-5-methylpyrrolidine | HCID 21278320 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | HCID 14326857 | HCID 14326857 | — |
반응 단계
Then, in substantially the same manner as in Example 9, 2.34 g of the thus obtained 1-(5-isoquinolinesulfonyl)-3-hydroxy-5-methylpyrrolidine was reacted in dichloromethane with 1.08 g of oxalyl chloride, 0.67 g of dimethylsulfoxide and 0.60 g of triethylamine to obtain 1-(5-isoquinolinesulfonyl)-5-methyl-3-pyrrolidone.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04798897 |
| 출처 데이터셋 | uspto-grants-1989_01 |
| ORD ID | ord-b459180677ee4d34ba8d53b34902e5e5 |
| 출처 메모 | uspto-grants-1989_01 |