HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Nicotinate → HCID 13672422, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Nicotinate | HCID 7151 | — |
| Reactant | 2,2,2-Trichloroethyl chloroformate | HCID 87063 | — |
| Reactant | 5-Methyl-2h-1,4-thiazin-3(4h)-one | HCID 290017 | — |
| Product | HCID 13672422 | HCID 13672422 | 48% |
Reaction Steps
A mixture of methylnicotinate (2.74 g), 2,2,2-trichloroethylchloroformate (3.44 ml) and 5-methyl-2H-1,4-thiazin-3(4H)-one (1.29 g) was treated in the same manner as described in Example 2 (i) to give the titled compound (2.1 g, yield 48%) as pale yellow crystals. Ethyl acetate-n-hexane (=1:1) was used as a developing eluant.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04800201 |
| Source dataset | uspto-grants-1989_01 |
| ORD ID | ord-53828ba992f14f64bad541748939520d |
| Source note | uspto-grants-1989_01 |