HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methylpyridine → HCID 13537834, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methylpyridine | HCID 7970 | — |
| Reactant | 2,2,2-Trichloroethyl chloroformate | HCID 87063 | — |
| Reactant | 5-Methyl-2h-1,4-thiazin-3(4h)-one | HCID 290017 | — |
| Product | HCID 13537834 | HCID 13537834 | 31% |
Reaction Steps
A mixture of 3-methylpyridine (0.72 g), 2,2,2-trichloroethylchloroformate (1.33 ml) and 5-methyl-2H-1,4-thiazin-3(4H)-one (0.5 g) was treated in the same manner as described in Example 2 (i) to give the titled compound (0.49 g, yield 31%) as milky white crystals. n-Hexane-ethyl acetate (=1:1) was used as a developing eluant.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04800201 |
| Source dataset | uspto-grants-1989_01 |
| ORD ID | ord-c0e30442669d4db5a6ed27fb6613ba5d |
| Source note | uspto-grants-1989_01 |