HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 14349734, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 13030113 | HCID 13030113 | — |
| Reactant | HCID 14349717 | HCID 14349717 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 14349734 | HCID 14349734 | 92.5% |
Reaction Steps
A mixture of 770 mg of (6R-trans)-3-[(acetyloxy)methyl]-7-[(aminothioxomethyl)amino]-8-oxo-5-thia-1-azabicyclo[4.2.0]oct-2-ene-2-carboxylic acid, diphenylmethyl ester, 425 mg of 3-bromo-2-oxopropanoic acid, trimethylsilyl ester, 110 mg of potassium carbonate and 15 ml of acetonitrile was reacted as described in Example 1, giving 810 mg of the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04800199 |
| Source dataset | uspto-grants-1989_01 |
| ORD ID | ord-ea003c55f8744cb0895ceed7ebe0a327 |
| Source note | uspto-grants-1989_01 |