HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 14257796, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 14257795 | HCID 14257795 | — |
| Solvent | Quinoline | HCID 7047 | — |
| Product | HCID 14257796 | HCID 14257796 | — |
Reaction Steps
The carboxylic acid from Step 1 (80 g, 0.37 mole) was dissolved in quinoline (750 mL) and Cu powder (16 g) was added to the solution. The reaction was heated to reflux for 90 min, cooled and 6N HCl (2L) was added. Extraction with EtOAc followed by chromatography on silica gel produced the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04800228 |
| Source dataset | uspto-grants-1989_01 |
| ORD ID | ord-ca7ae31c53884528a9f81a0224393cc4 |
| Source note | uspto-grants-1989_01 |