Water → HCID 86742686, compound

HRID 2292126Notes

Reaction equation

HRID 2292126 reaction equation
[CH2:1]([N:5]1[C:9](=[O:10])[N:8]([CH2:11][CH:12]2[O:14][CH2:13]2)[N:7]([CH2:15][CH:16]2[O:18][CH2:17]2)[C:6]1=[O:19])[CH:2]1[O:4][CH2:3]1.[OH2:20]>>[OH:20][CH:17]([OH:18])[CH2:16][CH2:15][N:7]1[C:6](=[O:19])[N:5]([CH2:1][CH:2]2[O:4][CH2:3]2)[C:9](=[O:10])[N:8]1[CH2:11][CH:12]1[O:14][CH2:13]1

Participants

3

Reactant 2

HCID 962WaterHCID 712181,2,4-Tris[(oxiran-2-yl)methyl]-1,2,4-triazolidine-3,5-dione

Product 1

HCID 86742686HCID 86742686, compound

Procedure

5 g of triglycidyl urazole (0.019 mole) are stirred for 3 hours at 70° C. in 50 ml of water. The solution is concentrated in a rotary evaporator and dried in a high vacuum. The colourless, oily crude product (5.8 g) is purified by column chromatography.

Workup

  1. concentrationThe solution is concentrated in a rotary evaporator
  2. customdried in a high vacuum
  3. customThe colourless, oily crude product (5.8 g) is purified by column chromatography

Sources & evidence

ORD record
ord-1777e503d263472a821782ce4a9aa754
Source dataset
uspto-grants-1989_01
Patent number
US04801601

Reaction notes

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