HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20070371, compound → 1-Propanol, 2-[(2-aminophenyl)amino]-2-methyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20070371 | HCID 20070371 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-Propanol, 2-[(2-aminophenyl)amino]-2-methyl- | HCID 11961557 | 98% |
Reaction Steps
N-(1-Hydroxy-2-methylprop-2-yl)-2-nitroaniline (10 g) in ethanol (200 ml) was hydrogenated over 5% palladium on charcoal (0.5 g) at 50 p.s.i. for 2 hours. The reaction was filtered and the solvent removed under vacuum to yield N-(1-hydroxy-2-methylprop-2-yl)benzene 1,2-diamine (8.4 g, 98%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04801598 |
| Source dataset | uspto-grants-1989_01 |
| ORD ID | ord-3fbe53d520414a24ac3a540c5bbe68f0 |
| Source note | uspto-grants-1989_01 |